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【ACE C18-PFP色譜柱】LC-MS/MS法檢測皮質(zhì)類固醇
ACE 3 C18-PFP: Corticosteroids by LC-MS/MS
ACE C18-PFP, 3μm, 150 x 2.1mm
Gradient analysis
A: 0.1% formic acid in water
B: CH3CN – 0.1% formic acid in water (90:10)
Time (mins) %B
0 30
14 50
17 95
20 30
Flow rate: 0.3ml/min
Column temperature: 15°C
Injection volume: 25μl
Turbospray, MRM
1. Triamcinolone
2. Prednisolone
3. Fluoroprednisolone
4. Methylprednisolone
5. Betamethasone
6. Dexamethasone
7. Flumethasone