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【ACE UltraCore SuperC18色譜柱】LC-MS/MS法檢測獸藥類固醇
Veterinary Steroids by LC-MS/MS
ACE UltraCore SuperC18, 2.5um, 100 x 2.1mm
Waters Acquity SDS system
Gradient analysis
A = 0.01mM amm. fluoride + 0.001% formic acid
B = Acetonitrile
Time (mins) %B Time (mins) %B
0 25 7.5 35
0.5 25 10.5 60
7.0 35
Flow rate: 0.5ml/min
Column temperature: 45°C
Positive or negative ESI MRM data
Also analysed in the same run (-ESI):
Taleranol and zeranol-d4
Taleranol and zeranol
Zearalenone
Hexestrol
Diethylstilbestrol
Dienestrol
Also analysed in the same run (+ESI):
Hydroxystanazolol
Hydroxystanazolol-d3
Methyltestosterone
Methyltestosterone-d3
β-Nortestosterone-d3
β-Trenbolone
α-Trenbolone