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【ACE UltraCore SuperC18色譜柱】LC-MS/MS法分析農(nóng)藥
Pesticides by LC-MS/MS
ACE UltraCore SuperC18, 2.5μm, 50 x 2.1mm
Gradient analysis
A = 0.1% HCOOH + 5mM NH4CO2H in 9:1 v/v H2O: MeOH
B = 0.1% HCOOH + 5mM NH4CO2H in 1:9 v/v H2O: MeOH
Flow Rate: 0.4ml/min
Temperature: 40°C
Injection volume: 20μl
Agilent 6420 Triple Quadrupole MS, +ve mode ESI Dynamic MRM
Also analysed under same conditions:
Acephate Hexaconazole
Acetamiprid Hexaflumuron
Aldicarb Imidacloprid
Aldicarb sulphone Indoxacarb
Aldicarb sulphoxide Mandipropamid
Benomyl Methamidophos
Carbendazim Methomyl
Carbofuran Monocrotophos
Clofentezine Nicotine
Clothianidin Omethoate
Cyfluthrin Oxamyl
Demeton S-methylsulphone Pencycuron
Demeton S-methylsulphoxide Prochloraz
Dicrotophos Propargite
Dimethoate Thiabendazole
Dinotefuran Thiacloprid
DMA Thiamethoxam
DMPF Thiodicarb
Flubendiamide Thiophanate methyl
Folpet Triforine
Formetanate
